++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
 +  XS  -  CRYSTAL STRUCTURE SOLUTION  - SHELXTL Ver. 6.12 W95/98/NT/2000/ME  +
 +  Copyright(c) 2001 Bruker AXS                         All Rights Reserved  +
 +  03srv164                              started at 14:41:51 on 26-Jul-2006  +
 ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++

 TITL S164 IN P2(1)/N
 CELL 0.71073 6.9196 14.5749 9.7248 90.0 90.637 90.0
 ZERR 4 0.0001 0.0002 0.0001 0.0 0.001 0.0
 LATT 1
 SYMM 0.500-X,0.500+Y,0.500-Z
 SFAC C H N F
 UNIT 40 40 16 8

 V =      980.71     At vol =    15.3     F(000) =     464.0     mu =   0.12 mm-1

 Max single Patterson vector =  27.8    cell wt =    896.88    rho =  1.519

 SIZE 0.36 0.18 0.10
 FVAR 0.36228
 TREF
  
 HKLF 4