[RSC Journal Format]

Experimental

Single crystals of %$xf.getFormula(html)% [%$spy.GetParam(snum.report.title)%] were recrystallised from [solvents] mounted in inert oil and transferred to the cold gas stream of the diffractometer.

Crystal structure determination of [%$spy.GetParam(snum.report.title)%]

Crystal Data. %$xf.getFormula(html)%, M =%3%, %1%, %$spy.getCellHTML()% U = %11% Å³, T = %27%, space group %$sg(%%h)% (no. %75%), Z = %16%, μ(Mo-Kα) = %19%, %29% reflections measured, %37% unique (R_int = %38%) which were used in all calculations. The final wR(F₂) was %54% (all data).

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